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Failures and Troubleshooting of a Rotary Evaporator - Rotovap

Failures and Troubleshooting of a Rotary Evaporator - Rotovap

Aug 08, 2019 A rotary evaporator is an indispensable equipment for evaporation, concentration, crystallization, drying, separation, and solvent recovery in many fields, and it is mainly used for continuous distillation of large amounts of volatile solvents under reduced pressure. Giving consideration to its importance, it’s necessary to learn something about …

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Bumping The Rotovap -

Bumping The Rotovap -

bumping. Remove and clean the bump bulb from the rotovap immediately after use to ensure ground glass joint connections do not stick together and to prevent contamination of future samples that will be rotovaped. 9. Always ensure that flasks, bump bulbs, and ground glass joint connections are secured

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Bumping In Rotovap -

Bumping In Rotovap -

bumping. Remove and clean the bump bulb from the rotovap immediately after use to ensure ground glass joint connections do not stick together and to prevent contamination of future samples that will be rotovaped. 9. Always ensure that flasks, bump bulbs, and ground glass joint connections are secured. Get Details

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Rotovap Distillation: What Is A Rotary Evaporator? -

Rotovap Distillation: What Is A Rotary Evaporator? -

Jul 21, 2017 A rotary evaporator or rotovap is an essential tool in a processing facility. Its primary use is in the recovery of ethanol after a winterization or extraction process. Although we’ll be focusing on how a rotovap operates during a basic ethanol recovery, know that it can be applied in the recovery of many other solvents that are compatible ...

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How to Minimize Bumping and Foaming Blog

How to Minimize Bumping and Foaming Blog

Jun 26, 2017 Bumping occurs when a sample boils rapidly, forming bubbles that cause the sample being concentrated to splash out of the flask. This is normally caused by heating too quick or applying too strong of a vacuum. The chances of it causing damage and splashes into the rotovap are increased if your evaporation flask is more than half full. Go slow, start with little …

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How to Speed Up Your Rotary Evaporation Process Blog

How to Speed Up Your Rotary Evaporation Process Blog

Jun 26, 2019 Using a rotovap is a crucial step in many processes as it enables you to gently and efficiently remove solvents from samples. In some cases, the rate of evaporation isn’t an issue, such as when you have very little solvent to evaporate or if time simply doesn't matter. ... Bumping: Bumping occurs when a sample boils too quickly and forms ...

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The Rotary Evaporator

The Rotary Evaporator

known as 'bumping - an intermittent, uncontrolled boiling. The on-off switch is located at the upper left on the rotovap motor and the speed control knob below it. You need not set the rotation speed of the flask at maximum; however, you must rotate the flask to prevent bumping at reduced pressure. 6. Lower the entire condenser-motor-flask ...

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An informative guide on a Rotovap - Rosin Power Blog

An informative guide on a Rotovap - Rosin Power Blog

Mar 05, 2020 Rotary evaporation requires a rotovap to rotate a flask under a vacuum. This rotation increases the surface area of the solvent, increases the rate of evaporation and reduces any chance of bumping. Since the process takes place in vacuum, it reduces the boiling point of solvent and provides a base for solvent extraction.

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Rotary Evaporator Bump Traps - Safety Emporium

Rotary Evaporator Bump Traps - Safety Emporium

Product Description. These are the most traditional rotary evaporator bump bulbs/traps which are used between the vapor tube and evaporation flask on a rotary evaporator to prevent the contents of the flask from being drawn into the condenser in the event of solvent bumping. The lower stem has 2 large holes; see CG-1321 and CG-1322 for modified ...

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Reducing Bumping on the Rotovap - BenchFly

Reducing Bumping on the Rotovap - BenchFly

Reducing Bumping on the Rotovap. by Alan Marnett. The bump guard lesson is usually learned one of two ways: A) someone teaches you, or B) someone doesn’t. The former is ideal and you may have no idea how lucky you are. The latter looks like this….

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Rotary Evaporator Bump Traps Chemglass - VWR

Rotary Evaporator Bump Traps Chemglass - VWR

Rotary Evaporator Bump Traps is used between the vapor tube and evaporation flask on a rotary evaporator to prevent contents of the flask from being drawn into the condenser in the event of bumping.Placing vacuum traps between an apparatus and vacuum source establishes a safe and controlled working system. The glassware protects the pump from the separated solvents …

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CG-1320 - ROTARY EVAPORATOR BUMP TRAPS

CG-1320 - ROTARY EVAPORATOR BUMP TRAPS

ROTARY EVAPORATOR BUMP TRAPS. AddThis. Used between the vapor tube and evaporation flask on a rotary evaporator to prevent contents of the flask from being drawn into the condenser in the event of “bumping.”. Traps have a 24/40 top outer joint and the listed size of lower inner joint. Bump Traps are available Plastic Coated.

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Rotovap Startup - csustan.edu

Rotovap Startup - csustan.edu

Rotovap Tips A. To avoid bumping: • Do not fill your flask full. • Faster spin rate usually helps. • Use a moderate bath temp – too high will cause excessively fast evaporation. B. Once you have removed the majority of solvent, empty the collection flask! • If you want to thoroughly dry the sample, reattach and continue ...

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Rotovaps The Buchwald Research Group

Rotovaps The Buchwald Research Group

Rotovaps. Rotavaps. To piss people off less, please remember that rotavaps are communal, and everyone is responsible for keeping them clean and functioning. This includes: 1. Emptying the collecting flask of solvent. Nobody should have to do it for you, and you know better than anyone what the collecting flask contains (EHS reminder).

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A Rotovap Archives - Rosin Power Blog

A Rotovap Archives - Rosin Power Blog

Sep 17, 2020 A Rotovap causes the spread of the thin film of warm solvent over a large surface. it happens because of the centrifugal force and the frictional force occurring between the wall of the rotating flask and the sample (generally liquid). These forces, an outcome of rotation, lead to suppressed bumping. These characteristics of the rotovap and the ...

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USA Lab 2L Rotovap Bump Trap Adapter 24/40 - USA Lab

USA Lab 2L Rotovap Bump Trap Adapter 24/40 - USA Lab

The USA Lab 2L bump trap is a convenient add on for your 2L rotovap. This product is designed to catch any splash back from your rotovap. For Technical Support, Questions, or Other Issues Please Email or Call Us!

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What Are Rotovaps and How Can They be Used?

What Are Rotovaps and How Can They be Used?

What is a rotovap? A rotary evaporator is a device used in chemical laboratories for the efficient and gentle removal of solvents from samples by evaporation. A rotovap acts like a filter to separate the unwanted components in the extract as a final step to crude oil. The rotovap is a simple concept with a lot of moving parts.

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Concentrating Extract in a Rotovap

Concentrating Extract in a Rotovap

While using a rotovap to concentrate the extract, it is essential to maintain the proper vacuum depth and flow rate to minimize process time and prevent sample loss through bumping or foaming. If the vacuum is too deep, product will evaporate with the solvent and bumping/over-boiling could be triggered.

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Title: Rotary Evaporator Page 1 of 6 ROTARY EVAPORATOR

Title: Rotary Evaporator Page 1 of 6 ROTARY EVAPORATOR

☐Note placed in front of the rotovap to indicate to others what chemicals are being used. ☐Solvent trap is emptied and bump trap is cleaned prior to use. ☐Bump trap and solvent trap are secured with metal or Keck clip.

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